Sulfuric acid, monobutyl ester → Butyl Acrylate

HRID 1721484Notes

Reaction equation

HRID 1721484 reaction equation
S(O)([O:4][CH2:5][CH2:6][CH2:7][CH3:8])(=O)=O.S([O-])([O:13][CH2:14][CH2:15][CH2:16]C)(=O)=O>>[C:14]([O:4][CH2:5][CH2:6][CH2:7][CH3:8])(=[O:13])[CH:15]=[CH2:16]

Participants

3

Reactant 2

HCID 70471Sulfuric acid, monobutyl esterHCID 4437320Butyl sulfate

Product 1

HCID 8846Butyl Acrylate

Procedure

The process is performed as in Reference Example 1, but arrangement is made for elimination of the butyl hydrogen sulphate by acid hydrolysis of the neutral butyl sulphate contained in the aqueous phase (A1). Experimentally, this reaction was carried out in two ways:

Sources & evidence

ORD record
ord-ebd994307dc7485fa31180a4d3777daa
Source dataset
uspto-grants-1996_04
Patent number
US05510514

Reaction notes

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