HCID 10105603, compound → 5-(5-Acetyl-2-furanyl)pentanol
Reaction equation
C([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]1[O:11][C:12]([C:15](=[O:17])[CH3:16])=[CH:13][CH:14]=1)(=O)C.C[O-].[Na+]>CO>[C:15]([C:12]1[O:11][C:10]([CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][OH:4])=[CH:14][CH:13]=1)(=[O:17])[CH3:16]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
5-(5-Acetyl-2-furanyl)pentanol acetate (60.6 g) was hydrolyzed with 3 g of sodium methoxide in 900 ml of absolute methanol and the product isolated to give 37.3 g of 5-(5-acetyl-2-furanyl)pentanol, b.p. 132°-135° C. (0.1 mm).
Workup
- customthe product isolated
Sources & evidence
- ORD record
- ord-d465b416f3704c29bb12436c3887e572
- Source dataset
- uspto-grants-1989_08
- Patent number
- US04861791
Reaction notes
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