Ethylamine → 4-Ethylamino-3-nitrobenzamide

HRID 1729581

Reaction equation

HRID 1729581 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1Cl)[C:7]([NH2:9])=[O:8])([O-:3])=[O:2].[CH2:14]([NH2:16])[CH3:15]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[NH:16][CH2:14][CH3:15])[C:7]([NH2:9])=[O:8])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 6341EthylamineHCID 279424-Chloro-3-nitrobenzamide

Product 1

HCID 37089224-Ethylamino-3-nitrobenzamide

Procedure

II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).

Workup

  1. temperatureThe mixture was cooled
  2. customthe precipitate was collected
  3. customcrystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product)

Sources & evidence

ORD record
ord-bb3097a7e15a44488e01fcb467723d81
Source dataset
uspto-grants-1976_11
Patent number
US03989522

Linked notes

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