Cyclohexyl propionate → HCID 15817998, compound
Reaction equation
C(O[CH:4]1[CH2:9][CH2:8][CH2:7][CH2:6][C:5]1=[O:10])C.[CH:11]1([O:17]C(=O)CC)CCCC[CH2:12]1.[H][H]>[Pd]>[CH2:11]([O:17][O:10][C:5]1[CH:4]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH3:12]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 10 gm. 2-ethoxycyclohexanone in 100 ml. cyclohexylpropionate was refluxed over 400 mg. of palladium on carbon until approximately 75% hydrogen had evolved. The catalyst was removed by filtration. O-ethoxyphenol was obtained in high yield.
Workup
- customThe catalyst was removed by filtration
Sources & evidence
- ORD record
- ord-ae19e5f7f1f54d7eb450cd8cda19c5c2
- Source dataset
- uspto-grants-1976_11
- Patent number
- US03992452
Reaction notes
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