Dimethylamine → HCID 20228668, compound
Reaction equation
[N:1]1[C:2]([C:10]2[CH:11]=[CH:12][C:13]3[S:17][C:16](=[O:18])[N:15]([CH3:19])[C:14]=3[CH:20]=2)=[CH:3][N:4]2[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=12.[CH2:21]=O.[CH3:23][NH:24][CH3:25]>>[CH3:23][N:24]([CH2:21][C:3]1[N:4]2[CH:9]=[CH:8][CH:7]=[CH:6][C:5]2=[N:1][C:2]=1[C:10]1[CH:11]=[CH:12][C:13]2[S:17][C:16](=[O:18])[N:15]([CH3:19])[C:14]=2[CH:20]=1)[CH3:25]Participants
4
Procedure
5-(3-Dimethylaminomethylimidazo[1,2-a]pyridin-2-yl)-3-methyl-2-benzothiazolinone (6.35 g) was prepared in substantially the same manner as that of Example 50 from 5-(imidazo[1,2-a]pyridin-2-yl)-3-methyl-2benzothiazolinone (8.86 g), 30% aqueous formaldehyde (2.57 g) and 50% aqueous dimethylamine (2.97 g).
Sources & evidence
- ORD record
- ord-ac77ffc40fdb42cbb210c05c1e690516