HCID 9795017, compound → HCID 13332658, compound

Reaction equation

[CH:1]1[C:11]2[CH:10]=[CH:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[S:6][C:5]=2[CH:4]=[C:3]([C:16](O)=[O:17])[CH:2]=1.C1C2CCC3C=CC=CC=3SC=2C=C(C(O)=O)C=1>>[OH:17][CH2:16][C:3]1[CH:2]=[CH:1][C:11]2[CH:10]=[CH:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[S:6][C:5]=2[CH:4]=1

Participants

Reactant 2

HCID 9795017HCID 9795017, compound

HCID 13151858HCID 13151858, compound

Product 1

HCID 13332658HCID 13332658, compound

Procedure

Repeat the process of Example 1, substituting an equivalent quantity of dibenzo[b,f]thiepin-3-carboxylic acid for the 10,11-dihydrodibenzo[b,f]thiepin-3-carboxylic acid, to obtain the title product (m.p., 111°-112° C.).

Sources & evidence

ORD record: ord-4a03b85d45c749948f4b1bc7f8b34646
Source dataset: uspto-grants-1980_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04237160

Reaction notes

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