Aniline → HCID 178526816, compound
Reaction equation
[OH:1][C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][N:5]=[C:4](SC)[N:3]=1.[NH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>C(O)C>[NH:13]([C:4]1[N:3]=[C:2]([OH:1])[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][N:5]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1Participants
4
Reagents, catalysts & solvents 1
Procedure
4.65 gm of 4-hydroxy-2-methylmercapto-5-nitropyrimidine (0.025 mol) are dissolved with heating in 150 ml of ethanol and refluxed for 5 hours with 4.68 gm of aniline (0.05 mol). The precipitated product is extracted in the cold, washed with ethanol and dried.
Workup
- extractionThe precipitated product is extracted in the cold
- washwashed with ethanol
- customdried
Sources & evidence
- ORD record
- ord-bee777dbd30a44bd92fc4b9edb4b28f5
- Source dataset
- uspto-grants-1980_12
- Patent number
- US04241056
Reaction notes
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