Reaction equation
[CH2:1]([C@:3]1([OH:28])[C:25]2[CH:24]=[C:23]3[N:10]([CH2:11][C:12]4[C:13]3=[N:14][C:15]3[CH:16]=[C:17]([F:22])[CH:18]=[CH:19][C:20]=3[CH:21]=4)[C:9](=[O:26])[C:8]=2[CH2:7][O:6][C:5](=[O:27])[CH2:4]1)[CH3:2].[CH3:29][CH:30]([CH3:35])[CH2:31][CH2:32]C=O>>[CH2:1]([C@:3]1([OH:28])[C:25]2[CH:24]=[C:23]3[N:10]([CH2:11][C:12]4[C:13]3=[N:14][C:15]3[CH:16]=[C:17]([F:22])[CH:18]=[CH:19][C:20]=3[C:21]=4[CH2:32][CH2:31][CH:30]([CH3:35])[CH3:29])[C:9](=[O:26])[C:8]=2[CH2:7][O:6][C:5](=[O:27])[CH2:4]1)[CH3:2]Participants
3
Reactant 2
Product 1
Procedure
The product of Example 2 is treated with 4-methylpentanal according to a procedure similar to Stage 13e in order to produce the expected solid.
Workup
- customto produce the expected solid
Sources & evidence
- ORD record
- ord-240de9541579496581056b41d5a60ae3
- Source dataset
- uspto-grants-2006_03
- Patent number
- US07012079B1
Linked notes
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