Sulfuric Acid → Lanthanum nitrate

HRID 1745868

Reaction equation

HRID 1745868 reaction equation
S(=O)(=O)(O)O.O.O.O.O.O.O.[N+:12]([O-:15])([O-:14])=[O:13].[La+3:16].[N+:17]([O-:20])([O-:19])=[O:18].[N+:21]([O-:24])([O-:23])=[O:22]>O>[N+:12]([O-:15])([O-:14])=[O:13].[La+3:16].[N+:17]([O-:20])([O-:19])=[O:18].[N+:21]([O-:24])([O-:23])=[O:22]

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 16211478Lanthanum nitrate hexahydrate

Product 1

HCID 25122Lanthanum nitrate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

NaY which had a SiO2/Al2O3 molar ratio of 5.0 in an amount of 235 g was suspended by stirring in 2000 g of pure water. To the resultant suspension was added dilute sulfuric acid to adjust the pH of the suspended slurry to 5.5. Aside therefrom, 246 g of lanthanum nitrate hexahydrate was dissolved in 500 g of warm water. The aqueous solution of lanthanum nitrate thus obtained was gradually mixed with the suspended slurry. Thereafter, the resultant mixture was heated to 90° C., stirred for 30 minutes, then filtered and washed. The washed cake was dried at 110° C. overnight, and calcined at 600° C. for 3 hours.

Sources & evidence

ORD record
ord-5e49a4c3d0c849e1bc89a7c0316ed183
Source dataset
uspto-grants-2006_03
Patent number
US07019183B2

Linked notes

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