HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyphenylboronic acid → 5-Formyl-6,2'-dimethoxy-biphenyl-3-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyphenylboronic acid | HCID 2733958 | — |
| Reactant | 3-Bromo-5-formyl-4-methoxy-benzenesulfonamide | HCID 86607698 | — |
| Product | 5-Formyl-6,2'-dimethoxy-biphenyl-3-sulfonamide | HCID 86607709 | 75.3% |
Reaction Steps
Proceeding as in Reference 19, but substituting 3-bromo-5-formyl-4-methoxy-benzenesulfonamide (0.9 g, 3.1 mmol) and 2-methoxybenzene boronic acid (0.51 g, 3.37 mmol), gave 5-formyl-6,2′-dimethoxy-biphenyl-3-sulfonamide (0.75 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09162986B2 |
| Source dataset | uspto-grants-2015_10 |
| ORD ID | ord-26a74c3c9b864501877cef1570022b14 |
| Source note | uspto-grants-2015_10 |