HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus sulfide (P2S5) → Tetradecanethioamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus sulfide (P2S5) | HCID 14817 | — |
| Reactant | Tetradecanamide | HCID 69492 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Tetradecanethioamide | HCID 21469509 | 191.5% |
Reaction Steps
Phosphorus pentasulfide (9.8 g, 0. 044 mol) was added to a mixture of tetradecanamide (8.6 g, 0.04 mol) in dry THF (250 mL) and the mixture refluxed overnight, concentrated in vacuo, and heated with methanol (200 mL), filtered, and the filtrate concentrated in vacuo to yield a pale yellow solid (10.28 g, 99%) used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05441975 |
| Source dataset | uspto-grants-1995_08 |
| ORD ID | ord-8cd84f54b5e94abc80f94e0245c86aa6 |
| Source note | uspto-grants-1995_08 |