Butanethiol → HCID 22769757, compound

Reaction equation

[CH3:1][S:2][CH:3]([C:11]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][CH:12]=1)[C:4]1[CH:9]=[CH:8][C:7]([Cl:10])=[CH:6][CH:5]=1.[CH2:18](S)[CH2:19][CH2:20]C>>[CH2:1]([S:2][CH:3]([C:4]1[CH:5]=[CH:6][C:7]([Cl:10])=[CH:8][CH:9]=1)[C:11]1[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][CH:12]=1)[CH2:18][CH2:19][CH3:20]

Participants

Reactant 2

HCID 8012Butanethiol

HCID 1770771,1'-[(Methylsulfanyl)methylene]bis(4-chlorobenzene)

Product 1

HCID 22769757HCID 22769757, compound

Procedure

The procedure described for making bis(p-chlorophenyl)methyl methyl sulfide was followed except that n-butyl mercaptan was used. The product obtained was greater than 90 percent pure.

Workup

customThe product obtained

Sources & evidence

ORD record: ord-522bb609616041129b36505d9734620e
Source dataset: uspto-grants-1978_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04117168

Reaction notes

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