Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitrobenzene | HCID 7416 | — |
| Reactant | Tetramethylammonium hydroxide dihydrate | HCID 22116808 | — |
| Solvent | Benzonitrile | HCID 7505 | — |
| Product | Azoxybenzene | HCID 10316 | 45% |
Reaction Steps
A solution containing 10 g of nitrobenzene, 1.27 g of tetramethylammonium hydroxide dihydrate and 1 g of benzonitrile was stirred at 60° C. with nitrogen bubbled into the solution via a syringe needle for 1 hour. Analysis of a sample of the reaction product by HPLC revealed N-(4-nitrophenyl)-benzamide was produced in 45% yield and azoxybenzene was generated in 22% yield based on tetramethylammonium hydroxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05380946 |
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| Source dataset | uspto-grants-1995_01 |
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| ORD ID | ord-a3dae9cde94f4c1a9997e15f107d85fd |
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| Source note | uspto-grants-1995_01 |
|---|
