Reaction equation
[Cl:1][C:2]1[CH:21]=[CH:20][C:5]([CH2:6][N:7]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[C:9]([C:16]([OH:19])([CH3:18])[CH3:17])=[N:8]2)=[C:4](C)[CH:3]=1.[Cl:23]C1C=C(Cl)C=CC=1CN1C2C(=CC=CC=2)C(C(OCC)=O)=N1>>[Cl:23][C:4]1[CH:3]=[C:2]([Cl:1])[CH:21]=[CH:20][C:5]=1[CH2:6][N:7]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:9]([C:16]([OH:19])([CH3:18])[CH3:17])=[N:8]1Participants
3
Procedure
The product was obtained using the method described for the preparation of compound 10b, but using as starting material compound 11a (0.4 mol) instead of compound 10a.
Workup
- customThe product was obtained
Sources & evidence
- ORD record
- ord-ccf0c7c70f5f4136beb3c28520b87e0d
- Source dataset
- uspto-grants-2016_02
- Patent number
- US09255073B2
Linked notes
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