1-Bromoheptane → 1-(4-Chlorophenyl)-3-heptyl imidazolium bromide

HRID 1774333Notes

Reaction equation

HRID 1774333 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)=[CH:4][CH:3]=1.[Br:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]>>[Br-:13].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N+:8]2[CH:12]=[CH:11][N:10]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:9]=2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 123691-BromoheptaneHCID 1428591-(4-Chlorophenyl)-1H-imidazole

Product 1

HCID 1784439481-(4-Chlorophenyl)-3-heptyl imidazolium bromide

Procedure

According to the general synthesis procedure, 5.6 mmol (1.00 g) 1-(4-chlorophenyl)imidazole and 6.7 mmol (1.20 g, 1.1 ml) 1-bromoheptane are dissolved in 5 ml TIE and heated for 12 h to 80° C.

Workup

  1. dissolutionare dissolved in 5 ml TIE
  2. temperatureheated for 12 h to 80° C.

Sources & evidence

ORD record
ord-a5749a2b076942a7808e3f26198f74b3
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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