Ethyl bromoacetate → Ethyl (2,3,5-trimethylphenoxy)acetate

Reaction equation

[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[CH:4][C:3]=1[OH:10].Br[CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14]>>[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([CH3:9])=[CH:4][C:3]=1[O:10][CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14]

Participants

Reactant 2

HCID 7748Ethyl bromoacetate

HCID 127692,3,5-Trimethylphenol

Product 1

HCID 28940153Ethyl (2,3,5-trimethylphenoxy)acetate

Procedure

Using 2,3,5-trimethylphenol and ethyl bromoacetate, the title compound was synthesized in the same manner as in Reference Example 153. Yield: quantitative. Oily matter.

Sources & evidence

ORD record: ord-ba9b7965008946d2ab79928044140f6f
Source dataset: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07507841B2

Reaction notes

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