n-Propylimidazole → HCID 178456359, compound

HRID 1789471

Reaction equation

HRID 1789471 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11]Cl)=[CH:4][CH:3]=1.[CH2:13]([N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)[CH2:14][CH3:15]>>[Cl-:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][N+:18]2[CH:19]=[CH:20][N:16]([CH2:13][CH2:14][CH3:15])[CH:17]=2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 118785n-PropylimidazoleHCID 200827321-Chloro-4-(4-chlorobutyl)benzene

Product 1

HCID 178456359HCID 178456359, compound

Conditions

Temperature
130 °C

Procedure

Add 7.13 g (0.035 mole) of 1-chloro-4-(4-chlorobutyl)benzene to 3.52 g (0.032 mole) of 1-propyl-1H-imidazole and heat to 130° C. for 18 hours. Follow the progress of reaction by NMR (CDCl3). At the completion of the reaction, cool to room temperature to obtain the title compound.

Workup

  1. customthe progress of reaction by NMR (CDCl3)
  2. customAt the completion of the reaction
  3. temperaturecool to room temperature

Sources & evidence

ORD record
ord-560edb78e0de42889fc1ab50fda17b06
Source dataset
uspto-grants-1987_08
Patent number
US04689341

Linked notes

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