2,4-Dichlorobenzylidenemalononitrile → HCID 10237507, compound

Reaction equation

[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[NH:7])=[CH:4][C:3]=1[O:11][CH3:12].[Cl:13][C:14]1[CH:25]=[C:24]([Cl:26])[CH:23]=[CH:22][C:15]=1[CH:16]=[C:17]([C:20]#[N:21])[C:18]#[N:19]>>[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]2[N:8]=[C:18]([NH2:19])[C:17]([CH2:20][NH2:21])=[C:16]([C:15]3[CH:22]=[CH:23][C:24]([Cl:26])=[CH:25][C:14]=3[Cl:13])[N:7]=2)=[CH:4][C:3]=1[O:11][CH3:12]

Participants

Reactant 2

HCID 180892,4-Dichlorobenzylidenemalononitrile

HCID 222206124-Amino-3-methoxybenzene-1-carboximidamide

Product 1

HCID 10237507HCID 10237507, compound

Procedure

The title compound, MS: m/e=389.9 (M+H+), was prepared from 4-amino-3-methoxy-benzamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

Sources & evidence

ORD record: ord-869275758913449eb22fc65c3a77c548
Source dataset: uspto-grants-2006_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07022718B2

Reaction notes

Loading…