Neopentyl glycol → 2-(5-Chlorothiophen-2-yl)-5,5-dimethyl-[1,3,2]dioxaborinane
Reaction equation
[Cl:1][C:2]1[S:6][C:5]([B:7]([OH:9])[OH:8])=[CH:4][CH:3]=1.[CH3:10][C:11]([CH2:15]O)([CH2:13]O)[CH3:12]>>[Cl:1][C:2]1[S:6][C:5]([B:7]2[O:9][CH2:12][C:11]([CH3:15])([CH3:13])[CH2:10][O:8]2)=[CH:4][CH:3]=1Participants
3
Procedure
The title compound (54%, crystals) was prepared from 5-chlorothiophen-2-boronic acid and neopentylglycol.
Sources & evidence
- ORD record
- ord-651969cc53834ff6ad060babc37b3893
- Source dataset
- uspto-grants-2006_05
- Patent number
- US07037905B2
Reaction notes
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