Neopentyl glycol → 2-(3-Bromophenyl)-5,5-dimethyl-1,3,2-dioxaborinane
Reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([B:8]([OH:10])[OH:9])[CH:5]=[CH:6][CH:7]=1.[CH3:11][C:12]([CH2:16]O)([CH2:14]O)[CH3:13]>>[Br:1][C:2]1[CH:3]=[C:4]([B:8]2[O:10][CH2:13][C:12]([CH3:16])([CH3:14])[CH2:11][O:9]2)[CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
The title compound (86%, crystals) was prepared from 3-bromophenylboronic acid and neopentylglycol.
Sources & evidence
- ORD record
- ord-885d7affc59848628a0f5325cf6fe033
- Source dataset
- uspto-grants-2006_05
- Patent number
- US07037905B2
Reaction notes
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