Sodium Hydroxide → HCID 22170839, compound

Reaction equation

[Cl:1][CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH2:12][C:13]([O:15]C)=[O:14])[CH:9]=[CH:10][CH:11]=1.[OH-].[Na+]>>[Cl:1][CH2:2][CH2:3][CH2:4][O:5][C:6]1[CH:7]=[C:8]([CH2:12][C:13]([OH:15])=[O:14])[CH:9]=[CH:10][CH:11]=1

Participants

Reactant 2

HCID 14798Sodium Hydroxide

HCID 22170468Methyl 2-[3-(3-chloropropoxy)phenyl]acetate

Product 1

HCID 22170839HCID 22170839, compoundYield 99.1%

Procedure

A mixture of methyl 2-[3-(3-chloropropoxy)phenyl]acetate (4.95 g, 0.02 moles) and a solution of 1N sodium hydroxide (0.02 moles) was stirred at room temperature for 24 hours. After acidification the acid separated as white powder (4.53 g, 97% yield)

Sources & evidence

ORD record: ord-0af6b850a1504ce99c4b90be42748f52
Source dataset: uspto-grants-2006_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07037929B1

Reaction notes

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