Pent-2-ene → 1-Decene
Reaction equation
[CH3:1][CH:2]=[CH:3][CH2:4][CH3:5]>[Ni]>[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:1][CH2:2][CH2:3][CH2:4][CH3:5]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
2-Pentene from the raffinate II metathesis was dimerized continuously as in example 2 over an Ni heterogeneous catalyst. Fractional distillation of the product gave a decene fraction with a purity of 99.5%.
Workup
- distillationFractional distillation of the product
Sources & evidence
- ORD record
- ord-14c1e55b18014b88ba06a48bac4578c9
- Source dataset
- uspto-grants-2006_06
- Patent number
- US07060852B2
Reaction notes
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