Methacrylic Acid → HCID 22051873, compound

HRID 1831024

Reaction equation

HRID 1831024 reaction equation
[C:1]([O:5][CH:6]=[CH2:7])([CH3:4])([CH3:3])[CH3:2].[C:8]([OH:13])(=[O:12])[C:9]([CH3:11])=[CH2:10]>>[C:8]([O:13][CH:6]([O:5][C:1]([CH3:4])([CH3:3])[CH3:2])[CH3:7])(=[O:12])[C:9]([CH3:11])=[CH2:10]

Participants

3

Reactant 2

HCID 4093Methacrylic AcidHCID 70220Propane, 2-(ethenyloxy)-2-methyl-

Product 1

HCID 22051873HCID 22051873, compound

Procedure

The reaction procedure of Example 1 was repeated using equimolar amounts of tert-butylvinyl ether and methacrylic acid. The structure of the product, 1-tert-butoxyethyl methacrylate (Compound D) was obtained in 79% yield. Compound D is an example of a mono-functional alpha-alkoxyalkyl(meth)acrylate which may optionally be included with multi-functional alpha-alkoxyalkyl(meth)acrylate compounds in compositions of the present invention. The structure of Compound D was confirmed by 1H NMR and infrared spectral analysis.

Workup

  1. customThe reaction procedure of Example 1

Sources & evidence

ORD record
ord-8c9f9f54bbcc41fca557c788284ec5fd
Source dataset
uspto-grants-2006_06
Patent number
US07067601B2

Linked notes

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