2-Butanamine, 1-methoxy- → [4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine

Participants

Role	Name	HCID	Charge
Reactant	2-Butanamine, 1-methoxy-	HCID 93837	—
Reactant	2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine	HCID 22052102	—
Product	[4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine	HCID 22052219	83%

Reaction Steps

2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine (0.25 g, 0.82 mmol) and 1-methoxymethyl-propylamine (0.23 g, 1.65 mmol) were treated substantially as described in Part D of Example 9 to produce 0.25 g (83%) of [4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine: MS (AP) m/z 370.2 [(M+H)+, 98].

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07067658B2
Source dataset	uspto-grants-2006_06
ORD ID	ord-e106ed2a922949afa1b2d417b551b5ba
Source note	uspto-grants-2006_06