3-Hydroxyacetophenone → 1-{3-[(5-Chloropentyl)oxy]phenyl)ethanone

Reaction equation

[OH:1][C:2]1[CH:3]=[C:4]([C:8](=[O:10])[CH3:9])[CH:5]=[CH:6][CH:7]=1.Br[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][Cl:17]>>[Cl:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][O:1][C:2]1[CH:3]=[C:4]([C:8](=[O:10])[CH3:9])[CH:5]=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 84873-Hydroxyacetophenone

HCID 960701-Bromo-5-chloropentane

Product 1

HCID 220487861-{3-[(5-Chloropentyl)oxy]phenyl)ethanone

Procedure

Prepared by Procedure U and Scheme AK using 1-(3-hydroxyphenyl)ethanone and 1-bromo-5-chloropentane.

Workup

customPrepared by Procedure U and Scheme AK

Sources & evidence

ORD record: ord-916eb5b6ee2942c0b997aeda47b915c5
Source dataset: uspto-grants-2006_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07067534B1

Reaction notes

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