1,4-Dibromobutane → HCID 68614413, compound

Reaction equation

[C:1]([O:5][C:6](=[O:16])[N:7]([C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1)[CH3:8])([CH3:4])([CH3:3])[CH3:2].[Br:17][CH2:18][CH2:19][CH2:20][CH2:21]Br>>[C:1]([O:5][C:6](=[O:16])[N:7]([C:9]1[CH:10]=[CH:11][C:12]([O:15][CH2:21][CH2:20][CH2:19][CH2:18][Br:17])=[CH:13][CH:14]=1)[CH3:8])([CH3:4])([CH3:2])[CH3:3]

Participants

Reactant 2

HCID 80561,4-Dibromobutane

HCID 54592515(4-Hydroxy-phenyl)-methyl-carbamic acid tert-butyl ester

Product 1

HCID 68614413HCID 68614413, compound

Procedure

In analogy to example 1.4, reaction of (4-Hydroxy-phenyl)-methyl-carbamic acid tert-butyl ester with 1,4-dibromobutane yielded [4-(4-Bromo-butoxy)-phenyl]-methyl-carbamic acid tert-butyl ester, MS: 360 (MH+, 1Br).

Sources & evidence

ORD record: ord-a5db07173ca3415c9ba5f1de544809ee
Source dataset: uspto-grants-2004_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06683201B2

Reaction notes

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