Reaction equation
[C:1]([O-:4])(=[O:3])[CH3:2].[K+:5].[C:6]([O-:9])(=[O:8])[CH3:7].[Na+:10]>COCCO>[C:1]([O-:4])(=[O:3])[CH3:2].[Na+:10].[K+:5].[C:6]([O-:9])(=[O:8])[CH3:7]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
In particular, for the preparation of the KNN solution, 0.87 g potassium acetate powder (CH3COOK) (Aldrich) and 0.73 g of sodium acetate powder (CH3COONa) (Aldrich) were dissolved separately in 10.6 mL of 2-methoxyethanol (2-MOE) solvent (Sigma-Aldrich). These two solutions were then mixed together to form a potassium-sodium acetate solution. Minor excesses of potassium acetate powder and sodium acetate powder were added into the potassium-sodium acetate solution to compensate for the loss of potassium and sodium during the subsequent heat treatment processes. 4 mL of niobium ethoxide ((CH3CH2O)5Nb) (Aldrich) was then added to the potassium-sodium acetate solution and dissolved completely to form a (K0.5Na0.5)NbO3 (KNN) solution.
Workup
- additionThese two solutions were then mixed together
Sources & evidence
- ORD record
- ord-ac99c7f1fb484ebb9b67df4504d3c1f6
- Source dataset
- uspto-grants-2015_02
- Patent number
- US08961679B2
Linked notes
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