Taurine → Carbobenzoxy-beta-alanyltaurine
Reaction equation
[N+](C1C=CC(O[C:11](=[O:25])[CH2:12][CH2:13][NH:14][C:15]([O:17][CH2:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[O:16])=CC=1)([O-])=O.[NH2:26][CH2:27][CH2:28][S:29]([OH:32])(=[O:31])=[O:30]>>[C:15]([NH:14][CH2:13][CH2:12][C:11]([NH:26][CH2:27][CH2:28][S:29]([OH:32])(=[O:31])=[O:30])=[O:25])([O:17][CH2:18][C:19]1[CH:20]=[CH:21][CH:22]=[CH:23][CH:24]=1)=[O:16]Participants
3
Procedure
1.9 g (5.5 mmoles) of N-carbobenzoxy-β-alanine-p-nitrophenyl ester (Biochemistry 4, 1884 1965) are reacted with 0.63 g (5 mmoles) of taurine as described in Example 1 to obtain 1.35 g (82%) of N-carbobenzoxy-β-alanyl-taurine.
Sources & evidence
- ORD record
- ord-be1229313538440b881240f50aef8d64
- Source dataset
- uspto-grants-1980_08
- Patent number
- US04218404