Trifluoroacetate → 6-methyl-4H,5H,6H,7H-thieno[2,3-c]pyridine-2-carboxylic acid
Reaction equation
[CH3:1][N:2]1[CH2:7][CH2:6][C:5]2[CH:8]=[C:9]([C:11]([O:13]C)=[O:12])[S:10][C:4]=2[CH2:3]1.FC(F)(F)C([O-])=O>>[CH3:1][N:2]1[CH2:7][CH2:6][C:5]2[CH:8]=[C:9]([C:11]([OH:13])=[O:12])[S:10][C:4]=2[CH2:3]1Participants
3
Procedure
Prepared analogously to Example 45b from methyl 6-methyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine-2-carboxylate (as the trifluoroacetate salt).
Sources & evidence
- ORD record
- ord-1a93376115ee4527ba01074e1bceeb63
- Source dataset
- uspto-grants-2012_11
- Patent number
- US08309542B2
Reaction notes
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