HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2,4-Dichlorophenyl)boronic acid → Methyl 5-(2,4-dichlorophenyl)-2-methyl-3-furoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2,4-Dichlorophenyl)boronic acid | HCID 2734659 | — |
| Reactant | Methyl 5-bromo-2-methylfuran-3-carboxylate | HCID 15534190 | — |
| Product | Methyl 5-(2,4-dichlorophenyl)-2-methyl-3-furoate | HCID 68514435 | 54% |
Reaction Steps
An operation similar to that in Example 49 (2) was performed using methyl 5-bromo-2-methyl-3-furoate (3.3 g) and 2,4-dichlorophenylboronic acid (3.4 g) to give the title compound (2.3 g, 54%) as a yellow crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08309580B2 |
| Source dataset | uspto-grants-2012_11 |
| ORD ID | ord-45891623dc0f40a39a4f542f3e57787f |
| Source note | uspto-grants-2012_11 |