2,3-Dichlorobenzeneboronic acid → HCID 178515768, compound

Reaction equation

C([O:8][C:9]1[N:14]=[C:13]2[NH:15][CH:16]=[N:17][C:12]2=[CH:11][CH:10]=1)C1C=CC=CC=1.[Cl:18][C:19]1[C:24]([Cl:25])=[CH:23][CH:22]=[CH:21][C:20]=1B(O)O>>[Cl:18][C:19]1[C:24]([Cl:25])=[CH:23][CH:22]=[CH:21][C:20]=1[N:15]1[C:13]2=[N:14][C:9]([OH:8])=[CH:10][CH:11]=[C:12]2[N:17]=[CH:16]1

Participants

Reactant 2

HCID 27346612,3-Dichlorobenzeneboronic acid

HCID 178420377HCID 178420377, compound

Product 1

HCID 178515768HCID 178515768, compound

Procedure

From 5-(benzyloxy)-3H-imidazo[4,5-b]pyridine and 2,3-dichlorophenylboronic acid, prepared in a similar manner as the one described in Example 1.26, the title compound was obtained. LCMS m/z=280.0 [M+H]+.

Sources & evidence

ORD record: ord-4312b57d0b7e4f5e902c43ef031aa690
Source dataset: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08507473B2

Reaction notes

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