tert-Butyl 4-(3-trimethylsilylprop-2-ynylidene)piperidin-1-carboxyate → 4-(3-Trimethylsilylprop-2-ynylidene)piperidine
Reaction equation
CC1C=CC=C(C#CC=C2CCNCC2)N=1.[CH3:17][Si:18]([CH3:36])([CH3:35])[C:19]#[C:20][CH:21]=[C:22]1[CH2:27][CH2:26][N:25](C(OC(C)(C)C)=O)[CH2:24][CH2:23]1>>[CH3:36][Si:18]([CH3:17])([CH3:35])[C:19]#[C:20][CH:21]=[C:22]1[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]1Participants
3
Procedure
The title compound was synthesized following the procedure described for the compound of Example 3 starting from Compound 2a instead of the Compound of Example 2.
Sources & evidence
- ORD record
- ord-bee8a9fb51ec4177bf41f8825546de94
- Source dataset
- uspto-grants-2013_08
- Patent number
- US08518916B2
Reaction notes
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