Methanol → Dimethyl Succinate

HRID 1903345

Reaction equation

[Na:1][Na].[CH3:3][O:4]C(C1[C:13](=[O:14])[CH2:12][CH:11]([C:15]([O:17][CH3:18])=[O:16])C(=O)C1)=O.[CH3:19][OH:20]>>[C:15]([O:17][CH3:18])(=[O:16])[CH2:11][CH2:12][C:13]([O:20][CH3:19])=[O:14].[CH3:3][O-:4].[Na+:1]

Participants

Reactant 3

HCID 887Methanol

HCID 948661,4-Cyclohexanedicarboxylic acid, 2,5-dioxo-, 1,4-dimethyl ester

HCID 141233Disodium

Product 2

HCID 7820Dimethyl Succinate

HCID 10942334Sodium Methoxide

Procedure

or dianilinodihydroterephthalic acids or the salts thereof, is characterised in that the suspension of the disodium salt of dimethyl succinylosuccinate, which suspension is obtained by condensation of dimethyl succinate in a 35-45 percent by weight solution of sodium methylate in methanol, is acidified, and the liberated dimethyl succinylosuccinate is condensed with at least 2 mols of a compound of the formula ##STR3## in which

Sources & evidence

ORD record: ord-73f2ea8408394a40b96a9c59cc6a489c
Source dataset: uspto-grants-1984_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04435589

Linked notes

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