Ethanone, 1-(3,5-bis(phenylmethoxy)phenyl)- → 3,5-Dibenzyloxyphenyl glyoxal

HRID 1906971Notes

Reaction equation

HRID 1906971 reaction equation
C([O:8]C1C=CC(C(=O)C)=CC=1CO)C1C=CC=CC=1.[CH2:20]([O:27][C:28]1[CH:29]=[C:30]([C:42](=[O:44])[CH3:43])[CH:31]=[C:32]([O:34][CH2:35][C:36]2[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=2)[CH:33]=1)[C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1>>[CH2:35]([O:34][C:32]1[CH:31]=[C:30]([C:42]([CH:43]=[O:8])=[O:44])[CH:29]=[C:28]([O:27][CH2:20][C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)[CH:33]=1)[C:36]1[CH:37]=[CH:38][CH:39]=[CH:40][CH:41]=1

Participants

3

Reactant 2

HCID 120098Ethanone, 1-(3,5-bis(phenylmethoxy)phenyl)-HCID 129693231-[3-(Hydroxymethyl)-4-(phenylmethoxy)phenyl]ethanone

Product 1

HCID 201341823,5-Dibenzyloxyphenyl glyoxal

Procedure

The title compound was prepared as a hydrate by the process of Description 54, replacing 1-(4-benzyloxy-3-hydroxymethylphenyl)ethanone. by 1-(3,5-dibenzyloxyphenyl)ethanone. γ (CDCl3) 6.40 (2H, s) 5.00 (4H, s), 2.40-3.50 (14H, m).

Sources & evidence

ORD record
ord-d1dc733ee75044848e3ea9b831200189
Source dataset
uspto-grants-1987_03
Patent number
US04654371

Reaction notes

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