Water → BPBA acetone

HRID 1927690

Reaction equation

HRID 1927690 reaction equation
[OH2:1].[CH2:2]([N:9]1[C:16](=[O:17])[CH:15]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:13](=[O:14])[NH:12][C:10]1=[O:11])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>CC(C)=O>[CH2:2]([N:9]1[C:16](=[O:17])[CH:15]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:13](=[O:14])[NH:12][C:10]1=[O:11])[C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1.[CH3:18][C:15]([CH3:16])=[O:1]

Participants

4

Reactant 2

HCID 962WaterHCID 1663402,4,6(1H,3H,5H)-Pyrimidinetrione, 5-phenyl-1-(phenylmethyl)-

Product 1

HCID 131729736BPBA acetone

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Separately, 40 g of distilled water and 6 g of acetone were added to a 200 mL beaker, and 17.29 g of 1-benzyl-5-phenylbarbituric acid (BPBA)(58.74 mmol) was added thereto and the mixture was dispersed homogeneously to obtain an aqueous BPBA/acetone solution.

Workup

  1. additionwas added
  2. additionthe mixture was dispersed homogeneously

Sources & evidence

ORD record
ord-580eb2e1026542f58dbb6ebd35bf98df
Source dataset
uspto-grants-2012_05
Patent number
US08183306B2

Linked notes

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