Tritylamine → HCID 57753550, compound

Reaction equation

Cl[CH2:2][C:3]1[C:8]([CH2:9]Cl)=[CH:7][C:6]([C:11]([F:14])([F:13])[F:12])=[CH:5][N:4]=1.[C:15]1([C:21]([NH2:34])([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[F:12][C:11]([F:14])([F:13])[C:6]1[CH:7]=[C:8]2[CH2:9][N:34]([C:21]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)([C:28]3[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=3)[C:22]3[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=3)[CH2:2][C:3]2=[N:4][CH:5]=1

Participants

Reactant 2

HCID 138598Tritylamine

HCID 577533602,3-Bis(chloromethyl)-5-(trifluoromethyl)pyridine

Product 1

HCID 57753550HCID 57753550, compound

Procedure

Prepared in analogy to Example A2 (b) from 2,3-Bis-chloromethyl-5-trifluoromethyl-pyridine and triphenylmethylamine. White solid. MS (m/e): 431.3 ([MH+, 100%).

Sources & evidence

ORD record: ord-290dc51c8fce47d0bd88dccad1229b6e
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08188139B2

Reaction notes

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