Ammonium Carbonate → HCID 53644843, compound
Reaction equation
[CH3:1][C:2]([CH3:20])([O:4][C:5]([NH:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][C:17](O)=[O:18])=[CH:11][CH:10]=1)=[O:6])[CH3:3].C(=O)([O-])[O-].[NH4+:25].[NH4+]>>[CH3:1][C:2]([CH3:20])([O:4][C:5]([NH:7][CH2:8][C:9]1[CH:14]=[CH:13][C:12]([CH2:15][CH2:16][C:17]([NH2:25])=[O:18])=[CH:11][CH:10]=1)=[O:6])[CH3:3]Participants
3
Procedure
Prepared analogously to Example 63a) from 4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzene propanoic acid, N,N'-carbonyldiimidazole and ammonium carbonate in a yield of 84% of theory. Colourless crystals, which were used in the following step without purification.
Workup
- customColourless crystals, which were used in the following step without purification
Sources & evidence
- ORD record