Thionyl Chloride → HCID 14985095, compound
Reaction equation
[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:18]=[CH:17][C:13]([C:14](O)=[O:15])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH2:2][CH3:3].S(Cl)([Cl:21])=O>C(Cl)Cl>[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:18]=[CH:17][C:13]([C:14]([Cl:21])=[O:15])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH2:2][CH3:3]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A mixture of 2.0 g of 4-(4-propylphenyl]benzoic acid and 30 ml of thionyl chloride is stirred at reflux for 45 minutes. The reaction mixture is evaporated in vacuo to a residue which is evaporated from carbon tetrachloride (2×50 ml) to give a residue which is dissolved in methylene chloride.
Workup
- temperatureat reflux for 45 minutes
- customThe reaction mixture is evaporated in vacuo to a residue which
- customis evaporated from carbon tetrachloride (2×50 ml)
- customto give a residue which
Sources & evidence
- ORD record
- ord-52f7bcafe5734851bda203c84335a920
- Source dataset
- uspto-grants-1998_07
- Patent number
- US05780471
Reaction notes
Loading…