Methanol → HCID 131714190, compound
Reaction equation
CO.Cl[Si:4](Cl)(Cl)[CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][N:8]=1>O>[SiH3:4][CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][N:8]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 2-(2-silylethyl)pyridine oligosilsesquioxane pillar material was prepared from a methanol solution of 2-(2-trichlorosilylethyl)pyridine (24 grams of 2-(2-trichlorosilylethyl)pyridine in 175 ml of methanol) by adding 10.5 ml of water. The mixture was stirred for 1 hour while maintaining the temperature below 30° C.
Workup
- temperaturewhile maintaining the temperature below 30° C.
Sources & evidence
- ORD record
- ord-3632116738ab40bdaa6d721e7104e28e
- Source dataset
- uspto-grants-1985_04
- Patent number
- US04510257
Reaction notes
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