Ethylamine → 2-Chloro-N-ethyl-5-hydroxybenzamide

HRID 1985991

Reaction equation

[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH2:12]([NH2:14])[CH3:13]>>[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][C:3]=1[C:4]([NH:14][CH2:12][CH3:13])=[O:6]

Participants

Reactant 2

HCID 6341Ethylamine

HCID 4582102-Chloro-5-hydroxybenzoic acid

Product 1

HCID 589074862-Chloro-N-ethyl-5-hydroxybenzamide

Procedure

The title compound was prepared from 2-chloro-5-hydroxybenzoic acid and ethylamine, using a method similar to that used for preparation 52, as a colourless solid.

Workup

customthat used for preparation 52, as a colourless solid

Sources & evidence

ORD record: ord-2cb6040aa4b94a889af74b84d652695e
Source dataset: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07547731B2

Linked notes

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