HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Benzyl-1-ethoxymethyl-3-methylxanthine → 1-Ethoxymethyl-3-methylxanthine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Benzyl-1-ethoxymethyl-3-methylxanthine | HCID 19689145 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Ethoxymethyl-3-methylxanthine | HCID 9815938 | — |
Reaction Steps
17.5 g (0.056 mol) of 7-benzyl-1-ethoxymethyl-3-methylxanthine were hydrogenated over 1.8 g of palladium (10%) on activated carbon at room temperature for 8 hours in 500 ml of ethanol. The catalyst was filtered off and the filtrate was concentrated to dryness and crystallized from dimethylformamide/diisopropyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728686 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-8274ed2fb34e4d4d9f44b77cbe179a49 |
| Source note | uspto-grants-1998_03 |