HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → 5-(Diethylphosphono)pentyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 5-Bromopentyl acetate | HCID 85140 | — |
| Product | 5-(Diethylphosphono)pentyl acetate | HCID 19689222 | — |
Reaction Steps
100.34 g (0.48 mol) of 5-bromopentyl acetate were heated at 150° C. for 8 hours with 79.8 g (0.048 mol) of triethyl phosphite while stirring and passing in nitrogen. The mixture was then fractionally distilled under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728686 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-37e8c73db5a4451484b91a4dd3cc9bb3 |
| Source note | uspto-grants-1998_03 |