HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → Diethyl 5-hydroxypentylphosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 5-(Diethylphosphono)pentyl acetate | HCID 19689222 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Diethyl 5-hydroxypentylphosphonate | HCID 10680635 | — |
Reaction Steps
92 g (0.345 mol) of 5-(diethylphosphono)pentyl acetate were heated at 50° C. for 10 hours with stirring with 74 g (0.7 mol) of finely powdered sodium carbonate in 500 ml of methanol. The solution was filtered, concentrated and distilled in a bulb tube.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728686 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-c88ff47b784b42e596807b91fc6e4cda |
| Source note | uspto-grants-1998_03 |