HCID 23235370, compound → HCID 66922426, compound

Reaction equation

[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][N:11]([C:14]([C:16]2[C:24]3[C:19](=[CH:20][N:21]=[CH:22][CH:23]=3)[N:18]([C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[C:17]=2Cl)=[O:15])[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[F:32][C:33]1[C:34]([CH3:41])=[C:35]([OH:40])[C:36]([CH3:39])=[CH:37][CH:38]=1>>[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][N:11]([C:14]([C:16]2[C:24]3[C:19](=[CH:20][N:21]=[CH:22][CH:23]=3)[N:18]([C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)[C:17]=2[O:40][C:35]2[C:36]([CH3:39])=[CH:37][CH:38]=[C:33]([F:32])[C:34]=2[CH3:41])=[O:15])[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 23235370HCID 23235370, compound

HCID 66922129HCID 66922129, compound

Product 1

HCID 66922426HCID 66922426, compound

Procedure

The title compound was prepared analogously as described in example 1, step 6, from the compound of example 16, step 5, (100 mg, 227 μmol) and 3-fluoro-2,6-dimethylphenol.

Sources & evidence

ORD record: ord-8b9db025e64842738812a1dbf8f016af
Source dataset: uspto-grants-2013_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08580813B2

Reaction notes

Loading…