Acetic Anhydride → HCID 53986315, compound

Reaction equation

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C@H:9]([OH:17])[CH2:10][C@H:11]2[CH2:15][CH2:14][CH2:13][N:12]2[CH3:16])[CH:6]=[CH:7][CH:8]=1.[C:18](OC(=O)C)(=[O:20])[CH3:19]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C@H:9]([O:17][C:18](=[O:20])[CH3:19])[CH2:10][C@H:11]2[CH2:15][CH2:14][CH2:13][N:12]2[CH3:16])[CH:6]=[CH:7][CH:8]=1

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 305435171157-63-6

Product 1

HCID 53986315HCID 53986315, compound

Procedure

According to the method of working described in Example 28, from 3.0 g of (R*,R*)-1-(3-methoxyphenyl)-2-(1-methyl-2-pyrrolidinyl)-ethanol and 30 ml of acetic acid anhydride there are obtained 1.56 g of the title compound as tough, colourless oil of b.p. 130° at 0.008 mm Hg.

Sources & evidence

ORD record: ord-d267f60654834e4ca9f32a95d5aa12b4
Source dataset: uspto-grants-1980_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04198424

Reaction notes

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