HCID 4763834, compound → HCID 4764068, compound
Reaction equation
[N+:1]([C:4]1[CH:17]=[CH:16][C:7]([NH:8][C:9]2[CH:10]=[C:11]([OH:15])[CH:12]=[CH:13][CH:14]=2)=[CH:6][CH:5]=1)([O-])=O>[C].[Pd]>[NH2:1][C:4]1[CH:17]=[CH:16][C:7]([NH:8][C:9]2[CH:10]=[C:11]([OH:15])[CH:12]=[CH:13][CH:14]=2)=[CH:6][CH:5]=1Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
20 Grams of 3-(4-nitroanilino)phenol was reduced under ordinary pressure in alcohol by the use of a palladium-carbon catalyst. After removing the catalyst by filtration, the alcohol was distilled off under reduced pressure and the residual solids were washed with benzene. The yield was 14 g, and melting point was 146°-149° C.
Workup
- customAfter removing the catalyst
- filtrationby filtration
- distillationthe alcohol was distilled off under reduced pressure
- washthe residual solids were washed with benzene
Sources & evidence
- ORD record
- ord-19510d727cd942f7830f05a204fe6628
- Source dataset
- uspto-grants-1980_04
- Patent number
- US04200466
Reaction notes
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