Ethyl propiolate → 1-(3-Oxoprop-1-EN-1-YL)aziridine-2-carbonitrile
Reaction equation
C(OCC)(=O)C#C.[C:8]([CH:10]1[CH2:12][N:11]1[CH:13]=[CH:14][C:15](OCC)=[O:16])#[N:9]>>[C:8]([CH:10]1[CH2:12][N:11]1[CH:13]=[CH:14][CH:15]=[O:16])#[N:9]Participants
3
Procedure
ethyl propiolate: ethyl 3-(2-cyanoaziridin-1-yl)-acrylate; oily substance, purified with a silica gel column; yield 24% of theory.
Workup
- customoily substance, purified with a silica gel column
Sources & evidence
- ORD record
- ord-5dd6fb68957f4f64bc5699ba01929ff5
- Source dataset
- uspto-grants-1982_03
- Patent number
- US04321194
Reaction notes
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