Benzoyl chloride, 3,4-dichloro- → HCID 21409861, compound
Reaction equation
[CH3:1][NH:2][CH2:3][C:4]1([N:10]2[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]2)[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1.[Cl:16][C:17]1[CH:18]=[C:19]([CH:23]=[CH:24][C:25]=1[Cl:26])[C:20](Cl)=[O:21]>C1C=CC=CC=1>[ClH:16].[CH3:1][N:2]([CH2:3][C:4]1([N:10]2[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]2)[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1)[C:20](=[O:21])[C:19]1[CH:23]=[CH:24][C:25]([Cl:26])=[C:17]([Cl:16])[CH:18]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Solutions of 1-[1-[(methylamino)methyl]cyclohexyl] piperidine (1.1 g., 0.005 mole) in dry benzene (25 ml) and 3,4-dichlorobenzoyl-chloride (1.0 g., 0.005 mole) in dry benzene (50 ml) were mixed and heated under reflux (steam bath) for 1 hr. The precipitate was filtered washed with benzene and dried. (1. 6 g.) m.p. 222° (dec.)