HCID 19855933, compound → HCID 19855920, compound
Reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[NH:10][C:11](=O)[CH2:12][N:13]([CH2:17][CH:18]1[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1)[CH2:14][CH:15]=[CH2:16].[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[NH:10][CH2:11][CH2:12][N:13]([CH2:17][CH:18]1[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]1)[CH2:14][CH:15]=[CH2:16]Participants
3
Procedure
In a manner similar to Preparation 2 react N-(2-chloro-4-methoxyphenyl)-2-[cyclohexylmethyl(2-propenyl)-amino]acetamide with lithium aluminum hydride to obtain the title compound.
Workup
- customIn a manner similar to Preparation 2
Sources & evidence
- ORD record
- ord-1dff0a6cd0d043769e44f013c8ff152f
- Source dataset
- uspto-grants-1990_04