Ethyl Spiro[2.5]octane-1-carboxylate → 2-Methylspiro[2.5]octane-1-carboxylic acid

HRID 2079468

Reaction equation

HRID 2079468 reaction equation
[CH3:1][CH:2]1[C:4]2([CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]2)[CH:3]1[C:10]([O:12]CC)=[O:11].C1(C(OCC)=O)C2(CCCCC2)C1>>[CH3:1][CH:2]1[C:4]2([CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]2)[CH:3]1[C:10]([OH:12])=[O:11]

Participants

3

Reactant 2

HCID 11206164Ethyl Spiro[2.5]octane-1-carboxylateHCID 67103119Ethyl 2-methylspiro[2.5]octane-1-carboxylate

Product 1

HCID 101035462-Methylspiro[2.5]octane-1-carboxylic acid

Procedure

The title compound was prepared as described in Example 1B substituting the product from Example 18A for the product from Example 1A. MS m/z 186 (M+NH4)+.

Sources & evidence

ORD record
ord-48055d8fa25e4982bcb6d4551c5cbc9b
Source dataset
uspto-grants-2011_04
Patent number
US07932245B2

Linked notes

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